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[Salinan]Disalin!
The sample (5 mg) was hydrolyzed (6 MHCl; 1 mL) in a
nitrogen atmosphere, for 12 h. The solution was filtered
through Whatman No. 1 and reduced in volume to dryness.
The residue was dissolved in a buffer solution (sodium
citrate, pH 2.20) and injected to a post column derivatizer
(Pickering Laboratories), adapted to a cation exchange column
(Na+, 8 lm, 3 mm ID · 250 mm) and a Perkin-Elmer
785 UV/VIS detector (570 nm
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