#Tips for NH3:When you get your gas

#Tips for NH3:

When you get your gas bottle of ammonia from BOC or other acetylene suppliers, get the associated mask and cartridges for NH3 and if a full face mask is too costly, use swimming goggles for the eyes., Always use gloves and cover up exposed skin, if you get skin burn just rinse it with water, and shower after a cook, you reek. Use a bathroom with a fan, open window for the main addition reaction. When getting liquid NH3 into erlenmeyer, tip tube upside down, stick a fitted pvc hose and empty 2.3 L of liquid into a dry plastic measuring flask. This way, you can measure abit more accurately, then tip NH3 into dry 4L erlenmeyer which is snug in a bucket of dry ice and tol or acetone half covering the ice, etc etc.

#Tips for additions:

Keep a plastic bag over the top of th 4L erlenmeyer to prevent dry ice, ice solvent(supercooling) whilst fitting it into the bucket system. Make sure stirrer is absolutely dry before dropping it into the flask. Add NH3 as described, activate stirrer, Add metal in and wait 20 minutes for it to dissolve, check, with a torch make sure it continues to stir and it all dissolves. Solution should turn dark blue to black and be really murky, if it stays clear add pre addition 200 ml solvent gently and this should help things along. Wait longer if you have to, success depends on all the metal dissolving. Just add more ice around the flask and keep it level near the top of the flask, push down occasionally on the dry ice because it forms gaps as it melts. Try not to add too much solvent to the dry ice as this will melt the ice quicker, have it 2/3 the way up the ice, this will take some rough calculation and observation. When confident of dissolution of all the metal, add pre addition solvent (200ml) gently. Then slowly drip pour the solvent with the freebase in it into the supercooled solution. Take regular pauses when the mist of ammonia rise out of the top of the erlenmeyer. On addition turn the stirrer up to a fast stirring pace. When pausing, cover top of flask covered with gloved hand or plastic bag and wait until mist goes and you can see solution again. Take your time at first, then make it quicker near the end - 20 minutes. Now total liquids in the flask are more than 4 L volume in a 4 L erl flask, why does it fit? Why is it so? Well the dry ice and solvent are keeping the solution between -38°C and -46°C so the density of the solvent occupies a somewhat smaller volume. Now that all the liquid additions are made, it's time to sprinkle the majority of the remaining freebase gently into the dark solution and turn up the stirrer to the safest fastest pace. The majority of the freebase in the solvent has already been converted to meth so there is lots of space for more to go in. After another 10-15 minutes the rest of the powdered freebase should be in the solution. Cover top and leave for 15-25 minutes. keep ice jacked up around flask. There should be 250 g of fb suzy in there to be converted.

#Tips for neutralisation and seperation:

Pull flask from ice with gloved hands and teatowells, this is cold...pour through dry strainer ( to catch undissolved Li or Na ) into clear square plastic bucket (like a 25L kids toy container, with lid from hardware store is ideal) that is immune to solvent. Do this with mask in a well ventilated room. throw any pieces of caught undissolved metal into a plastic bag. Tie up an flush down a friends toilet for a joke...Water additions create Naoh or LiOH but these whitish precipitates dissolve in water whilst your product stays in the upper solvent layer, so need not worry. Having no shiny bits that blow up floating on your dark mix makes slow water addition quite safe. I know from experience. Rinse erlenmeyer with 500 ml solvent, swirl and pour through strainer into main mix. Pour water in main mix and stir until solution turns clear and all whitish precipitates have dissolved. There is alot of ammonia smell steam from this. Leave covered for half to 1 hr then separate top solvent layer,dry by pouring in some oven dryed epsom saltsand stiring to pickup any residual water and pour through paper towel into a container to be crystallised. Flush NH3 water down toilet and most of your smell problem will be gone...

#Tips for crystallization with this:

Using one of those clear plastic buckets is ideal so you can keep glass down to a minimum, pour in solvent/freebase meth mix. Festers Hcl gas generator is ok, but we down under prefer to simplify it a bit. Pour 200 g non-iodised salt into a 2 L filtration flask, this flask has 2 ft length of clear ptfe hose on vac. nipple. Pour 98% sulfuric into a plastic pouring flask and pour 50 mls at a time onto salt and stopper. HCL gas immediately bubbles through solvent and creates NH3CL smoke which is harmless to breathe but gets quite thick. Watch bubbling froth in gas flask, tilt and swirl to reduce froth. Just unstopper, pour 50 ml acid and restopper quickly to keep it going. About 10 minutes roughly goes by and the only thing you generate is thick smoke from the surface of solvent. Keep going and after smoke generation dies down, crystals begin to form. Keep gassing until , white crystal layer begins to settle and alot of HCL gas rises from surface (you'll begin to smell it, do this with a fan and open window going...). Take vaccuum flask when finished and carefully pour water in to acid mix to neutralise it. Filter solvent, collect product and wash with a little solvent and gently dry crystals in a grill on a pyrex dish...etc You can retest the ether with litmus paper and if it still registers an alkali presence (turns blue), repeat procedure.

Please excuse the simplicity, but the KISS principal stands true. This is tried and tested and since 1997 is old news to us. 8 oz's of 14 - 1 100% pure is worth abit of money. If done twice, a lb is worth $42,000 in Victoria wholesale. Thats a bit of chemist travelling to get 300 boxes of 30's, at 10$ a box, which is the main expense, but who's complaining when you've paid off the house? It also keeps you independant from the main crews in the production deals so you don't have to fork out 50% for them supplying the ephedrine. Sell quickly, sell bulk C.O.D. and enjoy life. Independance is the key and soon this simplicity will be hampered with by authorities.

Yours independantly, Morph in Oz.

P.S. If you are left with smelly, wet or oily crystal, dissolve uncut into minimum water and boiloff in a pyrex dish, this will leave you with fairly dry immutable crystal "plates" that have to be scraped off.

Hasil (Melayu) 1:

#Tips bagi NH3:Apabila anda mendapatkan anda botol gas amonia daripada BOC atau lain-lain pembekal asetilena, dapatkan topeng bersekutu dan katrij untuk NH3 dan jika Topeng muka sepenuhnya adalah terlalu mahal, penggunaan renang merangkumi mata., sentiasa gunakan sarung tangan dan menutup kulit terdedah, jika anda dapat membakar kulit hanya membilasnya dengan air, dan pancuran mandian selepas Tukang masak, anda reek. Menggunakan bilik mandi dengan kipas angin, tingkap terbuka bagi tindak balas hebat yang utama. Apabila mendapat NH3 cecair ke dalam erlenmeyer, hujung tiub terbalik, melekat hos pvc dipasang dan kosongkan 2.3 L cecair ke dalam plastik yang kering mengukur flask. Dengan cara ini, anda boleh mengukur abit lebih tepat, kemudian Petua NH3 ke kering erlenmeyer 4L yang disampiri baldi ais kering dan tol atau acetone setengah merangkumi ais, dll dll.#Tips untuk tambahan:Keep a plastic bag over the top of th 4L erlenmeyer to prevent dry ice, ice solvent(supercooling) whilst fitting it into the bucket system. Make sure stirrer is absolutely dry before dropping it into the flask. Add NH3 as described, activate stirrer, Add metal in and wait 20 minutes for it to dissolve, check, with a torch make sure it continues to stir and it all dissolves. Solution should turn dark blue to black and be really murky, if it stays clear add pre addition 200 ml solvent gently and this should help things along. Wait longer if you have to, success depends on all the metal dissolving. Just add more ice around the flask and keep it level near the top of the flask, push down occasionally on the dry ice because it forms gaps as it melts. Try not to add too much solvent to the dry ice as this will melt the ice quicker, have it 2/3 the way up the ice, this will take some rough calculation and observation. When confident of dissolution of all the metal, add pre addition solvent (200ml) gently. Then slowly drip pour the solvent with the freebase in it into the supercooled solution. Take regular pauses when the mist of ammonia rise out of the top of the erlenmeyer. On addition turn the stirrer up to a fast stirring pace. When pausing, cover top of flask covered with gloved hand or plastic bag and wait until mist goes and you can see solution again. Take your time at first, then make it quicker near the end - 20 minutes. Now total liquids in the flask are more than 4 L volume in a 4 L erl flask, why does it fit? Why is it so? Well the dry ice and solvent are keeping the solution between -38°C and -46°C so the density of the solvent occupies a somewhat smaller volume. Now that all the liquid additions are made, it's time to sprinkle the majority of the remaining freebase gently into the dark solution and turn up the stirrer to the safest fastest pace. The majority of the freebase in the solvent has already been converted to meth so there is lots of space for more to go in. After another 10-15 minutes the rest of the powdered freebase should be in the solution. Cover top and leave for 15-25 minutes. keep ice jacked up around flask. There should be 250 g of fb suzy in there to be converted.#Tips for neutralisation and seperation:Pull flask from ice with gloved hands and teatowells, this is cold...pour through dry strainer ( to catch undissolved Li or Na ) into clear square plastic bucket (like a 25L kids toy container, with lid from hardware store is ideal) that is immune to solvent. Do this with mask in a well ventilated room. throw any pieces of caught undissolved metal into a plastic bag. Tie up an flush down a friends toilet for a joke...Water additions create Naoh or LiOH but these whitish precipitates dissolve in water whilst your product stays in the upper solvent layer, so need not worry. Having no shiny bits that blow up floating on your dark mix makes slow water addition quite safe. I know from experience. Rinse erlenmeyer with 500 ml solvent, swirl and pour through strainer into main mix. Pour water in main mix and stir until solution turns clear and all whitish precipitates have dissolved. There is alot of ammonia smell steam from this. Leave covered for half to 1 hr then separate top solvent layer,dry by pouring in some oven dryed epsom saltsand stiring to pickup any residual water and pour through paper towel into a container to be crystallised. Flush NH3 water down toilet and most of your smell problem will be gone...#Tips for crystallization with this:Using one of those clear plastic buckets is ideal so you can keep glass down to a minimum, pour in solvent/freebase meth mix. Festers Hcl gas generator is ok, but we down under prefer to simplify it a bit. Pour 200 g non-iodised salt into a 2 L filtration flask, this flask has 2 ft length of clear ptfe hose on vac. nipple. Pour 98% sulfuric into a plastic pouring flask and pour 50 mls at a time onto salt and stopper. HCL gas immediately bubbles through solvent and creates NH3CL smoke which is harmless to breathe but gets quite thick. Watch bubbling froth in gas flask, tilt and swirl to reduce froth. Just unstopper, pour 50 ml acid and restopper quickly to keep it going. About 10 minutes roughly goes by and the only thing you generate is thick smoke from the surface of solvent. Keep going and after smoke generation dies down, crystals begin to form. Keep gassing until , white crystal layer begins to settle and alot of HCL gas rises from surface (you'll begin to smell it, do this with a fan and open window going...). Take vaccuum flask when finished and carefully pour water in to acid mix to neutralise it. Filter solvent, collect product and wash with a little solvent and gently dry crystals in a grill on a pyrex dish...etc You can retest the ether with litmus paper and if it still registers an alkali presence (turns blue), repeat procedure.
Please excuse the simplicity, but the KISS principal stands true. This is tried and tested and since 1997 is old news to us. 8 oz's of 14 - 1 100% pure is worth abit of money. If done twice, a lb is worth $42,000 in Victoria wholesale. Thats a bit of chemist travelling to get 300 boxes of 30's, at 10$ a box, which is the main expense, but who's complaining when you've paid off the house? It also keeps you independant from the main crews in the production deals so you don't have to fork out 50% for them supplying the ephedrine. Sell quickly, sell bulk C.O.D. and enjoy life. Independance is the key and soon this simplicity will be hampered with by authorities.

Yours independantly, Morph in Oz.

P.S. If you are left with smelly, wet or oily crystal, dissolve uncut into minimum water and boiloff in a pyrex dish, this will leave you with fairly dry immutable crystal "plates" that have to be scraped off.

Hasil (Melayu) 2:

#Tips Untuk NH3:. Apabila anda mendapat botol gas anda ammonia daripada BOC atau pembekal asetilena lain, dapatkan topeng dan kartrij yang berkaitan untuk NH3 dan jika topeng muka penuh adalah terlalu mahal, gogal penggunaan renang untuk mata, Sentiasa gunakan sarung tangan dan menutup kulit yang terdedah, jika anda mendapatkan kulit membakar hanya membilasnya dengan air, dan mandi selepas tukang masak, anda berbau. Gunakan bilik mandi dengan kipas, tingkap yang terbuka bagi tindak balas penambahan utama. Apabila mendapat cecair NH3 ke Erlenmeyer, tiub hujung terbalik, berpegang hos pvc dipasang dan kosong 2.3 L cecair ke dalam pengukur plastik kering kelalang. Dengan cara ini, anda boleh mengukur abit lebih tepat lagi, kemudian hujung NH3 ke kering 4L Erlenmeyer yang nyaman dalam baldi ais kering dan tol atau aseton separuh meliputi ais, dan lain-lain dan lain-lain #Tips untuk penambahan: Pastikan beg plastik lebih atas daripada ke 4L Erlenmeyer untuk mengelakkan ais kering, ais pelarut (supercooling) semasa pemasangan ke dalam sistem baldi. Membuat pengacau pasti sememangnya kering sebelum menjatuhkan ke dalam kelalang. Tambah NH3 seperti yang dinyatakan, mengaktifkan pengacau, Tambah logam dan tunggu 20 minit untuk itu untuk membubarkan, cek, dengan obor memastikan ia terus kacau dan semuanya larut. Penyelesaian perlu bertukar menjadi biru gelap kepada hitam dan menjadi benar-benar keruh, jika itu akan tetap jelas menambah Selain pra 200 ml pelarut perlahan-lahan dan ini akan membantu perkara-perkara bersama-sama. Menunggu lebih lama jika anda perlu, kejayaan bergantung pada semua melarutkan logam. Hanya menambah lebih banyak ais sekitar kelalang dan menyimpannya tahap berhampiran bahagian atas kelalang, tolak ke bawah kadang-kadang di atas ais kering kerana ia membentuk jurang kerana ia cair. Cuba untuk tidak menambah terlalu banyak pelarut untuk ais kering kerana ini akan mencairkan ais lebih cepat, mempunyai ia 2/3 jalan sehingga ais, ini akan mengambil sedikit pengiraan kasar dan pemerhatian. Apabila yakin pembubaran semua logam, tambah pra pelarut tambahan (200ml) perlahan-lahan. Kemudian perlahan-lahan menitis tuangkan pelarut dengan Freebase di dalamnya ke dalam penyelesaian supercooled. Ambil menjeda biasa apabila kabus ammonia keluar daripada bahagian atas Erlenmeyer itu. Di samping itu bertukar kacau sehingga kadar kacau yang cepat. Apabila berhenti, tutup bahagian atas kelalang ditutup dengan tangan bersarung getah atau beg plastik dan tunggu sehingga kabut pergi dan anda boleh melihat penyelesaian lagi. Ambil masa anda pada mulanya, kemudian menjadikannya lebih cepat berhampiran akhir - 20 minit. Kini jumlah cecair dalam kelalang lebih daripada 4 L jumlah dalam 4 L ERL kelalang, mengapa ia patut? Mengapa begitu? Well ais kering dan pelarut menyimpan penyelesaian di antara -38 ° C dan -46 ° C supaya ketumpatan pelarut menduduki jumlah yang agak kecil. Sekarang semua penambahan cecair yang dibuat, ia adalah masa untuk taburkan majoriti Freebase baki perlahan-lahan ke dalam penyelesaian yang gelap dan hadir kacau kepada kadar yang paling selamat terpantas. Majoriti Freebase dalam pelarut telah memeluk meth jadi terdapat banyak ruang untuk masuk ke dalam. Selepas 10-15 minit lagi seluruh Freebase serbuk seharusnya berada di dalam penyelesaian. Tutup bahagian dan biarkan selama 15-25 minit. menjaga ais menaikkan sekitar kelalang. Perlu ada 250 g fb suzy di sana untuk ditukar. #Tips Untuk peneutralan dan pemisahan: Tarik kelalang dari ais dengan tangan bersarung getah dan teatowells, ini adalah sejuk ... tuangkan melalui tapisan kering (untuk menangkap larut Li atau Na) ke dalam baldi jelas persegi plastik (seperti 25L bekas mainan kanak-kanak, dengan tudung dari kedai perkakasan sesuai) yang kebal kepada pelarut. Adakah ini dengan topeng di dalam bilik pengudaraan yang baik. membuang mana-mana kepingan logam larut ditangkap ke dalam beg plastik. Mengikat siram yang turun tandas rakan-rakan untuk jenaka ... penambahan air mewujudkan NaOH atau LiOH tetapi ini mendakan putih larut dalam air manakala produk anda kekal dalam lapisan pelarut atas, jadi tidak perlu risau. Tidak mempunyai bit berkilat yang meletupkan terapung di atas campuran gelap anda membuat tambahan air perlahan agak selamat. Saya tahu dari pengalaman. Bilas Erlenmeyer dengan 500 ml pelarut, pusaran dan tuangkan melalui penapis ke dalam campuran utama. Tuangkan air dalam campuran utama dan kacau sehingga penyelesaian ternyata jelas dan semua mendakan putih telah dibubarkan. Terdapat banyak daripada bau ammonia wap daripada ini. Cuti dilindungi untuk setengah hingga 1 jam kemudian lapisan atas berasingan pelarut, kering dengan menuang dalam beberapa ketuhar dryed Epsom saltsand stiring untuk pickup apa-apa air sisa dan tuangkan melalui tuala kertas ke dalam bekas yang akan dilontarkan. Siram air NH3 ke dalam tandas dan kebanyakan masalah bau anda akan hilang ... #Tips untuk penghabluran dengan ini: Dengan menggunakan salah satu baldi plastik yang jelas adalah sesuai supaya anda boleh menyimpan kaca ke minimum, tuangkan campuran meth / Freebase pelarut . Festers Hcl penjana gas ok, tetapi kita lebih suka ke bawah di bawah untuk memudahkan sedikit. Tuangkan 200 g garam bukan beriodin ke dalam 2 L penapisan kelalang, kelalang ini mempunyai 2 panjang ft hos PTFE jelas mengenai vac. puting. Tuangkan 98% sulfurik ke dalam mencurah kelalang plastik dan tuangkan 50 mls pada satu masa ke garam dan penyumbat. Gas HCL segera buih melalui pelarut dan mencipta NH3CL asap yang tidak berbahaya untuk bernafas tetapi mendapat agak tebal. Menonton menggelegak buih di dalam kelalang gas, sendeng dan pusaran untuk mengurangkan buih. Hanya unstopper, tuangkan 50 ml asid dan restopper dengan cepat untuk memastikan ia berterusan. Kira-kira 10 minit lebih kurang berlalu dan satu-satunya perkara yang anda menghasilkan asap tebal dari permukaan pelarut. Teruskan usaha dan selepas generasi asap meninggal dunia turun, kristal mula terbentuk. Menjaga pembunuhan sehingga, lapisan kristal putih bermula untuk menyelesaikan dan alot gas HCL naik dari permukaan (anda akan mula bau, lakukan ini dengan kipas angin dan tingkap yang terbuka akan ...). Ambil vaccuum flask apabila selesai dan berhati-hati tuangkan air dalam campuran asid untuk meneutralkan itu. Menapis pelarut, mengumpul produk dan basuh dengan pelarut sedikit dan kristal perlahan-lahan kering di grill pada hidangan pyrex ... dan lain-lain Anda boleh menguji semula eter dengan kertas litmus dan jika ia masih mendaftarkan kehadiran alkali (bertukar biru), prosedur berulang. sila maafkan kesederhanaan, tetapi ibu KISS berdiri benar. Ini dicuba dan diuji dan sejak 1997 adalah berita lama kepada kami. 8 oz sebanyak 14-1 100% tulen bernilai abit wang. Jika dilakukan dua kali, lb yang bernilai $ 42,000 di Victoria borong. Thats sedikit ahli kimia perjalanan untuk mendapatkan 300 kotak 30-an, 10 $ kotak, yang merupakan perbelanjaan utama, tetapi yang mengadu apabila anda telah berhasil rumah? Ia juga membolehkan anda sentiasa Independant dari krew utama dalam tawaran pengeluaran supaya anda tidak perlu membayar 50% untuk mereka membekalkan ephedrine. Menjual dengan cepat, menjual pukal COD dan menikmati kehidupan. Kemerdekaan adalah kunci dan tidak lama lagi kesederhanaan ini akan terjejas dengan pihak berkuasa. Yours secara bebas, Morph dalam Oz. PS Jika anda ditinggalkan dengan berbau, basah atau berminyak kristal, membubarkan dipotong ke dalam air minimum dan boiloff dalam pinggan Pyrex, ini akan meninggalkan anda agak kering berubah kristal "plat" yang perlu dikikis.