Red Phosphorous/Iodine Methamphetam

Red Phosphorous/Iodine Methamphetamine Synthesis
by Placebo
Ok, this is an amalgamation of many peoples methods! I beleive this to be the best, simplest, fastest, and cleanest method for producing meth-amphetamine, in the highest yeilds possible for RP/I2/E reaction! Remember, each and every step gives small losses, and this method has the least steps! It is a culmination of efforts by, Worlock, CHEMMAN, and maybe a few tiny touches by me! I re-iterate, I don't want any congratulations except for the write-up itself!

You will need these things, and no substitutions allowed! If you can't get this shit, you aint ready to make the best Go-Go in town! This is a refinement of all methods, and the next step up from Push Pull, But nobody should be dicouraged from attempting this, as you will probably find it easier! PH paper, isn't even necessary!

This post is one method from Go to Whoah! This post has to be followed from GO to Whoah! Otherwise you can run into trouble, as povidone is not removed in this extraction! It will be removed at the end! Each step was chosen to compliment the next! Understand?

Equipment
Various jars
2L pyrex vessel
2L 2 neck round flat bottom flask
1 condenser, I reccomend a coil condenser but a liebig will suffice!
1 sloping splashhead or better still, a steam distillation sloping splashhead!
A steam pressure cooker, that has releif valve at top
Hotplate, electric of course!
Filter paper, Bucner and vacuum would be nice too!
thermometer
1 glass stopper
lengths of clear pvc tubing
Pot with vegetable oil, that can fit your reaction vessel
Reagents (All must be clean and anhydrous!)
Iodine crystals
Red Phosphorous
Pseudo-ephedrine, or ephedrine
Methanol
Toluene
Acetone
NaOH
Ice
Extraction of pfed
Ok, this method will deal with the Hcl salt of pfed, and a streamlined version of "the cure"! All pills are dumped into a large jar and double the volume of methanol poured on top! This is stirred vigourously and let to settle, in the fridge seems to speed it up! After top methanol layer has cleared it is carefully decanted off. This procedure is repeated 3 times. All methanol pulls are put together and reduced on a hotplate. As methanol gets down to last little bit, it is taken off heat Then a portion of acetone, twice your remaing liquid is dropped in. This forces the pfed crystals to crash out. Then remaining liquid is carefully evaped off.

Now you have your crude/dirty pfed Hcl. Next we will be doing successive toluene washes So put your pfed crystals in a pyrex (heat proof glass) Now add toluene to a safe level that can be lightly boiled on hotplate After about 5 mins boiling with stirring. Take off heat and let settle a minute. Now carefully pour off toluene into a filter to catch any remnants of pfed that may follow. Now if you get the toluene that has our contaminents in it and add some water You will see the crap crash from the toluene into the water This is the crap that came thru with the methanol pull!

So as we continue to do multiple toluene washes, We will continue to test the toluene after pouring it off, To see how we are progressing with the cleanup! When we have reached a point where no crap comes out of the toluene, With the addition of water, then we are ready to try acetone! Usually about 3 boils in toluene, but of course it depends how much your using! So, as before we will add a portion of acetone and boil lightly! Now when we pour off the acetone, we will add a tiny amount of water and some NaOH This is our final test, when you do this and no crap falls out of acetone you are ready!

This will be the cleanest pfed you have ever seen, guarenteed! AND, yeilds should be >90% if your careful! 95% is good.

Reaction
Smallest reaction to be attempted, especially by newbees, is 1oz of pfed! So that even taking into account sloppiness, lack of experience and losses along the way You should get some product!

Ratios of reagents are, 3:3:1 or 1:1:1/3 ie.E:I:RP aka, equal amounts of Iodine and pfed, and a third as much RP! Comprenda!

Ok first prepare yourself an icebath! Yes icecubes and water in a sink or bucket! Now, many will say you should add this first or that first! Well after much reading of different peoples methods, I say.... Chuck the whole shebang in together, while your flask is on ice, Lift and swirl ingredients together, while maintaing on ice! Put your condenser on top and start water running thru, from bottom to top! Now, the idea is to get the reaction going in the most controlled way possible. Now you want to let reagents react in the icebath, if at all, Then move vessel from icebath to room temp, If things look like they're going too fast, put back in ice bath, You want to keep the reaction going but only at a nice slow, controlled pace! This is also necessary to control vapour in the condenser! Thick and or dis-colored smoke is bad! and plumes of smoke will escape from condenser As things progress at a nice slow pace, as things slow too much you can start applying heat! So prepare an oilbath and bring to about 50c, now if there is no more action in your vessel You can move it to the oilbath, and same as before, when things slow down, Adjust heat up, to say 100c then 150c for one hour, to make sure reaction has completed The whole time you should be watching to keep a nice reflux going, and not too much vapour is escaping from condenser!

Now remove from heat and disconnect condenser, Now add ice water to quench reaction, reason for ice water is to calm the reaction down when NaOH is added Now its up to you if you want to filter out RP or leave till the end I would leave it, it will be washed nicely by next process and be easier to filter! Now add lots of NaOH to bring reaction mix to positive 14PH You cannot over-basify as meth won't be destroyed, its a tough MF!

Steam Distillation
Now you need to set up your glassware for steam distillation! So attach steam distillation sloping splashhead to top hole of flask! Now attach plastic hose to steam inlet and other end, on release valve of pressure cooker that is full of water! Now attach condenser on end of splashhead, and rig up some kind of prop for it to stay up! Now place a jar at the end of condenser to catch our distillate! Now you want to heat both the pressure cooker, and the reaction flask! Now sit back and get ready for one of the most beautiful sites and smells! The meth freebase that is sitting on the top of your aqueous layer in flask will vapourise and be carried across and be condensed in the condenser and trickle down into your jar It will sit atop a bottom layer of water! After the last of the oil has come across, change jars and leave the setup to run for another hour Just to make sure you got it all! Any povidone from the pills will be stuck behind in the reaction vessel It has been noted that some polymer that may have been left from extraction, may follow the steam!

Crystallisation
So, now we have a jar of water, with this sweet clear oil sitting on top! Now options are to add Hcl acid slowly with stirring until oil layer disappears and then evap the whole lot to get crystals! Or, as I found, you may have some polymer that has come over with the steam and is now sitting in the water layer, and it looks cloudy! So I don't want to evap all that, it will just concentrate the shit in there (plus its very time consuming evapping water, plus you risk losing some meth as the water evaps) So, I think you should just throw a little toluene into jar, and then seperate! Now your absolutly pure meth freebase is in your toluene! Now you can either gas, for instant clean meth, or Add minimal DH2O and then acidify to PH7, shake, seperate and evap water for crystals! repeat this step if you do it this way, as some more may come in second go!

Now with this process from start to finish, you shouldn't need to re-crystallise As your product should be the cleanest shit anybody has ever seen anyway! But you may want to for the purpose of growing nice big crystals! In which case, add just enough hot methanol to dissolve all your meth and then place in freezer. The secret is, the slower the evap, the bigger the crystals! So a nice slow room temp evap over several days might be fun!

Enjoy, and do not attempt anything above, before you completely understand what you are doing! You must have a sound understanding of the basics first!

Hasil (Melayu) 1:

Merah fosforus/iodin Methamphetamine sintesisoleh plaseboOK, ini adalah percantuman di banyak kaedah rakyat! Saya percaya ini merupakan kaedah terbaik, termudah, terpantas dan menzahirkan untuk menghasilkan meth-sini, di yeilds tertinggi yang mungkin bagi reaksi Mata Ganjaran/I2/E! Ingatlah, setiap langkah memberikan kerugian kecil, dan kaedah ini mempunyai langkah-langkah yang paling! Ia adalah kemuncak daripada usaha oleh, Worlock, CHEMMAN, dan mungkin sedikit kecil sentuhan oleh saya! Saya semula iterate, saya tidak mahu sebarang tahniah kecuali penulisan itu sendiri!Anda akan memerlukan perkara-perkara ini, dan tiada penggantian dibenarkan! Jika anda tidak boleh mendapatkan tahi ini, anda tidak sedia untuk membuat yang terbaik Go-Go di bandar! Ini adalah sebagai penapisan semua kaedah dan langkah seterusnya sehingga dari tolak tarik, tetapi tiada siapa yang harus dicouraged dari cubaan ini, kerana anda mungkin akan mendapati ia lebih mudah! Kertas PH, tidak perlu pun!Posting ini adalah satu kaedah dari pergi ke Whoah! Posting ini telah disusuli dari pergi ke Whoah! Sebaliknya anda boleh menghadapi kesusahan, seperti povidone tidak dialih keluar dalam pengekstrakan ini! Ia akan dikeluarkan pada akhir! Setiap langkah telah dipilih untuk memuji seterusnya! Faham?PeralatanBalang yang pelbagaiKapal pyrex 2L2L 2 leher bulat flask bawah flat1 condenser, saya cadangkan condenser gegelung tetapi liebig yang memadai!1 splashhead condong atau masih lebih baik, splashhead condong Penyulingan Stim!Periuk tekanan Wap, yang mempunyai injap releif di atasHotplate, elektrik sudah tentu!Kertas turas, Bucner dan vakum akan lebih baik juga!termometerpenyumbat kaca 1panjang tiub pvc jelasPeriuk dengan minyak sayuran, yang boleh memuatkan kapal reaksi andaReagan (semua mestilah bersih dan kontang!)Iodin KristalFosforus merahAlkaloid pseudo, atau alkaloidMetanolTolueneAcetoneNaOHAisPengekstrakan pfedOK, kaedah ini akan berurusan dengan garam Hcl dari pfed, dan versi yang diperkemas untuk "sembuh"! Semua pil akan dibuang ke dalam sebuah balang besar dan dua kali ganda jumlah metanol dicurahkan di atas! Ini adalah vigourously dikacau dan biarkan untuk menjelaskan, dalam peti sejuk seolah-olah mempercepatkan ia! Selepas lapisan atas metanol telah dibersihkan adalah dengan teliti decanted off. Prosedur ini adalah diulang 3 kali. Semua metanol berbalas akan meletakkan bersama-sama dan dikurangkan atas hotplate yang. Seperti metanol mendapat ke lepas sedikit, ia diambil dari haba maka sebahagian daripada acetone, dua kali cecair remaing anda jatuh pada. Ini memaksa Kristal pfed untuk kemalangan keluar. Kemudian baki cecair dimatikan dengan berhati-hati evaped.Sekarang anda mempunyai pfed mentah/kotor anda Hcl. Seterusnya kita akan melakukan washes toluene berturut-turut supaya meletakkan Kristal pfed anda dalam sebuah pyrex (kaca haba bukti) kini menambah toluene hingga ke paras yang selamat yang boleh menjadi ringan direbus pada hotplate selepas kira-kira 5 minit mendidih dengan dikacau. Mengambil daripada haba dan biarkan menyelesaikan seminit. Kini dengan teliti Tuang off toluene ke dalam penapis untuk menangkap sebarang sisa-sisa pfed yang boleh diikuti. Sekarang jika anda mendapat toluene yang contaminents kami di dalamnya dan tambah sedikit air, anda akan melihat kemalangan omong kosong dari toluene itu ke dalam air ini adalah omong kosong yang datang melalui dengan tarik metanol!Jadi kami terus melakukan pelbagai toluene washes, kami akan terus menguji toluene itu selepas mencurah, untuk melihat bagaimana kita akan berjalan lancar dengan pembersihan! Apabila kita telah sampai ke titik di mana crap tidak datang daripada toluene, dengan air, maka kami bersedia untuk mencuba acetone! Biasanya kira-kira 3 bisul toluene, tetapi sudah tentu ia bergantung berapa banyak anda menggunakan! Jadi, kerana sebelum ini kami akan menambah sebahagian acetone dan rebus sedikit! Sekarang bila kita Tuang off acetone ini, kita akan menambah sejumlah kecil air dan beberapa NaOH yang ini adalah ujian akhir kami, apabila anda melakukan ini dan omong kosong tiada jatuh daripada acetone anda sudah bersedia!Ini akan menjadi yang menzahirkan pfed anda pernah lihat, guarenteed! DAN, yeilds harus > 90% jika anda berhati-hati! 95% adalah baik.Tindak balasReaksi yang terkecil untuk dicuba, terutama sekali oleh newbees, adalah 1oz pfed! Supaya lebih mengambil kira akaun sloppiness, kekurangan pengalaman dan kerugian duka anda perlu mendapatkan beberapa produk!Nisbah ini penting untuk berada, 3:3:1 atau 1:1:1 / 3 iaitu. E: saya: Mata Ganjaran aka, sama dengan jumlah iodin dan pfed, dan ketiga sebesar Mata Ganjaran! Comprenda!OK terlebih dahulu mempersiapkan diri anda untuk icebath! Ya icecubes dan air di sinki atau baldi! Sekarang, ramai yang akan berkata anda patut menambah pertama ini atau itu dahulu! Selepas banyak membaca kaedah berlainan bangsa, saya katakan... Membuang shebang keseluruhan di bersama-sama, ketika flask anda sedang ais, Lif dan swirl bahan bersama, sementara maintaing pada ais! Meletakkan condenser anda di atas dan mula berjalan air thru, dari bawah ke atas! Sekarang, Ideanya adalah untuk mendapatkan tindak balas yang berlaku dalam cara yang Tempahan terkawal. Kini anda hendak membenarkan untuk bertindak balas dalam icebath, sama sekali, kemudian mengalih kapal dari icebath ke bilik temp, jika perkara-perkara yang kelihatan seperti mereka akan terlalu cepat, masukkan semula dalam mandian ais, anda mahu mengekalkan tindak balas akan tetapi hanya pada yang bagus perlahan, kawalan kelajuan! Ianya juga perlu untuk mengawal wap di condenser itu! Asap tebal dan dis-berwarna adalah buruk! dan plumes asap akan terlepas daripada condenser sebagai keadaan kemajuan pada baik lambat kelajuan, perkara-perkara yang lambat terlalu banyak yang anda boleh mula menggunakan haba! Jadi oilbath untuk menyedia dan membawa kepada kira-kira 50c, kini jika ada tiada tindakan lanjut di kapal anda, anda boleh memindahkan ia oilbath ini, dan sama seperti dahulu, apabila perkara-perkara yang melambatkan, melaraskan memanaskan, katakan 100c kemudian 150c selama satu jam, untuk memastikan tindak balas telah selesai sepanjang masa anda harus dapat menonton perlu berterusan refluks bagus , dan tidak terlalu banyak wap melarikan diri dari condenser!Kini mengalih keluar dari haba dan putuskan condenser, sekarang Tambah air ais untuk menghilangkan tindak balas, sebab air ais adalah untuk menenangkan reaksi turun Bilakah NaOH ditambah kini terpulang kepada anda jika anda mahu untuk menapis Mata Ganjaran atau meninggalkan pertunjukan saya akan meninggalkan ia, ia akan dibasuh baik oleh proses seterusnya dan akan lebih mudah untuk penapis! Sekarang Tambah banyak NaOH membawa reaksi campuran ke 14PH positif yang anda tidak boleh terlalu basify sebagai meth tidak dimusnahkan, ia adalah sebuah MF sukar!Penyulingan StimSekarang, anda perlu sediakan barangan kaca anda untuk Penyulingan Stim! Jadi lampirkan splashhead condong penyulingan wap ke atas lubang flask! Kini melampirkan hos plastik kepada wap inlet dan hujung satu lagi, pada injap keluaran daripada periuk tekanan yang penuh dengan air! Kini melampirkan condenser pada penghujung splashhead, dan pelantar sehingga beberapa jenis prop untuk bangun! Sekarang letakkan balang yang pada penghujung condenser untuk menangkap sulingan kami! Sekarang anda mahu memanaskan kedua-dua periuk tekanan, dan flask tindak balas! Kini bercuti dan bersedialah untuk salah satu laman yang paling cantik dan bau! Freebase meth yang duduk di bahagian atas lapisan anda air dalam flask akan vapourise dan dibawa merentasi dan pekat di condenser dan meleleh turun ke dalam balang anda ia akan duduk atas lapisan bawah air! Lepas minyak sesudah datang di seberang, Tukar balang dan meninggalkan persediaan untuk bertanding lagi jam hanya untuk memastikan anda mendapat semua! Povidone apa-apa dari pil akan terperangkap di belakang dalam kapal tindak balas tersebut ia telah diperhatikan bahawa beberapa polimer yang boleh ditinggalkan daripada pengekstrakan, boleh ikut stim!CrystallisationSo, now we have a jar of water, with this sweet clear oil sitting on top! Now options are to add Hcl acid slowly with stirring until oil layer disappears and then evap the whole lot to get crystals! Or, as I found, you may have some polymer that has come over with the steam and is now sitting in the water layer, and it looks cloudy! So I don't want to evap all that, it will just concentrate the shit in there (plus its very time consuming evapping water, plus you risk losing some meth as the water evaps) So, I think you should just throw a little toluene into jar, and then seperate! Now your absolutly pure meth freebase is in your toluene! Now you can either gas, for instant clean meth, or Add minimal DH2O and then acidify to PH7, shake, seperate and evap water for crystals! repeat this step if you do it this way, as some more may come in second go!Now with this process from start to finish, you shouldn't need to re-crystallise As your product should be the cleanest shit anybody has ever seen anyway! But you may want to for the purpose of growing nice big crystals! In which case, add just enough hot methanol to dissolve all your meth and then place in freezer. The secret is, the slower the evap, the bigger the crystals! So a nice slow room temp evap over several days might be fun!Enjoy, and do not attempt anything above, before you completely understand what you are doing! You must have a sound understanding of the basics first!